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dc.contributor.authorHinokuma, Satoshi
dc.contributor.authorWiker, Geir
dc.contributor.authorSuganuma, Takuya
dc.contributor.authorBansode, Atul
dc.contributor.authorStoian, Dragos
dc.contributor.authorHuertas, Silvia Caminero
dc.contributor.authorMolina, Sonia
dc.contributor.authorShafir, Alexandr
dc.contributor.authorRønning, Magnus
dc.contributor.authorVan Beek, Wouter
dc.contributor.authorUrakawa, Atsushi
dc.date.accessioned2019-03-21T14:10:10Z
dc.date.available2019-03-21T14:10:10Z
dc.date.created2018-05-04T13:03:35Z
dc.date.issued2018
dc.identifier.citationEuropean Journal of Inorganic Chemistry. 2018, 2018 (17), 1847-1853.nb_NO
dc.identifier.issn1434-1948
dc.identifier.urihttp://hdl.handle.net/11250/2591121
dc.description.abstractUnderstanding the physicochemical origin of functional materials generally requires multifaceted information on their material characteristics, which are investigated by various analytical methods. In this respect, a simultaneous multiprobe approach to studying materials by complementary methods is of great value, particularly following dynamically varying processes, such as chemical and structural transformations under reactive environments. Herein, we report facile and versatile approaches to combining synchrotron X‐ray absorption spectroscopy and X‐ray diffraction with IR spectroscopy, in transmission and diffuse‐reflection sampling configurations, to study pellet samples under controlled environments. The high practicality of the approach is enabled by the use of a modular IR spectrometer. Rich information on the chemical, electronic, and structural changes of Zr–BTC and Cu–BTC MOFs during thermal treatment has been gained by the multiprobe approach. The advantages and practical challenges of the combined approaches are discussed.nb_NO
dc.language.isoengnb_NO
dc.publisherWileynb_NO
dc.titleVersatile IR spectroscopy combined with synchrotron XAS–XRD: Chemical, electronic, and structural insights during thermal treatment of MOF materialsnb_NO
dc.typeJournal articlenb_NO
dc.typePeer reviewednb_NO
dc.description.versionacceptedVersionnb_NO
dc.source.pagenumber1847-1853nb_NO
dc.source.volume2018nb_NO
dc.source.journalEuropean Journal of Inorganic Chemistrynb_NO
dc.source.issue17nb_NO
dc.identifier.doi10.1002/ejic.201800140
dc.identifier.cristin1583494
dc.description.localcodeThis is the peer reviewed version of an article, which has been published in final form at https://doi.org/10.1002/ejic.201800140. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Self-Archiving.nb_NO
cristin.unitcode194,66,30,0
cristin.unitnameInstitutt for kjemisk prosessteknologi
cristin.ispublishedtrue
cristin.fulltextpostprint
cristin.qualitycode1


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