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Synthesis of [13C4]-labeled ∆9-tetrahydrocannabinol and 11-nor-9-carboxy-∆9-tetrahydrocannabinol as internal standards for reducing ion supressing/alteration effects in LC/MS-MS quantification
(Journal article; Peer reviewed, 2014)(−)-Δ9-Tetrahydrocannabinol is the principal psychoactive component of the cannabis plant and also the active ingredient in some prescribed drugs. To detect and control misuse and monitor administration in clinical ... -
Synthesis of a (Ti, Mo)B<inf>2</inf> coating by electro-codeposition in NaCl–KCl–AlCl<inf>3</inf>–MoO<inf>3</inf> melt containing TiB<inf>2</inf> nanoparticles
(Peer reviewed; Journal article, 2022)This paper demonstrates the availability of electro-codeposition (i.e., the simultaneous occurrence of electrophoretic deposition of nanoparticles and electrochemical deposition of metal ions) in molten salts without the ... -
Synthesis of a Novel Benzoyl Adenosine Analog Containing a 1, 4-Dioxane Sugar Analog and the Synthesis of a Corresponding Uracil Adenine Dinucleotide
(Journal article; Peer reviewed, 2011)Adenosine analogs in which the sugar unit was replaced by a 1,4-dioxane sugar equivalent, were prepared by coupling the 1,4-dioxane sugar analog as its anomeric acetates, with N6-benzoyl protected adenine. The 1,4-dioxane ... -
Synthesis of alkali-silica reaction product structurally identical to that formed in field concrete
(Peer reviewed; Journal article, 2020)Alkali-silica reaction (ASR) can cause expansion and cracking of concrete. Despite significant progress over the past 80 years, the molecular structures of the ASR products remain poorly understood. These reaction products ... -
Synthesis of asymmetric movement trajectories in timed rhythmic behaviour by means of frequency modulation
(Journal article; Peer reviewed, 2017)Results from different empirical investigations on gestural aspects of timed rhythmic movements indicate that the production of asymmetric movement trajectories is a feature that seems to be a common characteristic of ... -
Synthesis of CO‐tolerant Ni‐Pt Rhombic Dodecahedra Bimetallic Electrocatalytic Nanoparticles
(Peer reviewed; Journal article, 2020)Developing scalable synthetic routes for fabricating low‐cost CO‐tolerant and highly active electrocatalysts have significant relevance for fuel cell applications. Here, we report a novel and rapid single step synthesis ... -
Synthesis of Crosslinked PEG/IL Blend Membrane via One-Pot Thiol–Ene/Epoxy Chemistry
(Journal article, 2020)Poly(ethylene glycol) (PEG)-based membranes have obtained considerable attentions for CO2 separation for their promising CO2 separation performance and excellent thermal/ chemical resistance. In this work, a one-pot ... -
Synthesis of Crosslinked PEG/IL Blend Membrane via One-Pot Thiol–Ene/Epoxy Chemistry
(Journal article, 2020)Poly(ethylene glycol) (PEG)-based membranes have obtained considerable attentions for CO2 separation for their promising CO2 separation performance and excellent thermal/ chemical resistance. In this work, a one-pot ... -
A synthesis of feasible control methods for floating offshore wind turbine system dynamics
(Journal article, 2021)During the past decade, the development of offshore wind energy has transitioned from near shore with shallow water to offshore middle-depth water regions. Consequently, the energy conversion technology has shifted from ... -
Synthesis of glycoconjugates utilizing the regioselectivity of a lytic polysaccharide monooxygenase
(Peer reviewed; Journal article, 2020)Polysaccharides from plant biomass are the most abundant renewable chemicals on Earth and can potentially be converted to a wide variety of useful glycoconjugates. Potential applications of glycoconjugates include therapeutics ... -
Synthesis of Heat-Integrated Water Networks with exergo-economic criteria
(Peer reviewed; Journal article, 2023)This paper considers the exergy analysis of Heat-Integrated Water Networks (HIWNs) rarely addressed in the literature. Two objective functions were analyzed, with the first minimizing the total annualized cost (TAC) and ... -
Synthesis of Hollow Silica Nanospheres by Sacrificial Polystyrene Templates for Thermal Insulation Applications
(Journal article; Peer reviewed, 2013)Monodisperse polystyrene (PS) spheres with controllable size have been synthesized by a straight forward and simple procedure. The as-synthesized PS spheres have a typical diameter ranging from ~180 nm to ~900 nm, where a ... -
Synthesis of hydrides by interaction of intermetallic compounds with ammonia
(Journal article; Peer reviewed, 2015)Interaction of intermetallic compounds with ammonia was studied as a processing route to synthesize hydrides and hydridonitrides of intermetallic compounds having various stoichiometries and types of crystal structures, ... -
Synthesis of Hydroxy Sulfonate Surfactants
(Journal article; Peer reviewed, 2005)The selective synthesis of sulfonate surfactants with side chains containing ether- and hydroxy groups was carried out using cyclic sulfates as epoxide analogues. The main chain was elaborated from 1,2-dodecane sulfate ... -
Synthesis of magnesium complexes of ionic liquids with highly coordinating anion
(Journal article; Peer reviewed, 2019)Magnesium(II) complexes, [Mg2+(hfac−)3][Cation+], were prepared as solids from hydrophobic hexafluoroacetylacetonate ionic liquids ([Cation+][hfac−] ILs) and Mg(Tf2N)2. 1-Butyl-3-methylimidazolium ([C4mim]), N-butylpyridinium ... -
Synthesis of Novel 3,6-Dithienyl Diketopyrrolopyrrole Dyes by Direct C‒H Arylation
(Peer reviewed; Journal article, 2020)Direct C-H arylation coupling is potentially a more economical and sustainable process than conventional cross-coupling. However, this method has found limited application in the synthesis of organic dyes for dye-sensitized ... -
Synthesis of Novel Homo-N-Nucleoside Analogs Composed of a Homo-1,4-Dioxane Sugar Analog and Substituted 1,3,5-Triazine Base Equivalents
(Journal article; Peer reviewed, 2008)Enantioselective syntheses from dimethyl tartrate of 1,3,5-triazine homo-Nnucleoside analogs, containing a 1,4-dioxane moiety replacing the sugar unit in natural nucleosides, were accomplished. The triazine heterocycle ... -
Synthesis of polynucleotide analogs containing a polyvinyl alcohol backbone
(Journal article; Peer reviewed, 2008)Water soluble homo-base polynucleotide analogues were synthesized in which polyvinyl alcohol and partially phosphonated polyvinyl alcohol constituted the backbones, onto which were grafted uracil or adenine via 1,3-dioxane ... -
Synthesis of PVA/CeO2 based nanocomposites with tuned refractive index and reduced absorption edge: Structural and optical studies
(Peer reviewed; Journal article, 2021)n the current study, polymer nanocomposites (NCPs) based on poly (vinyl alcohol) (PVA) with altered refractive index and absorption edge were synthesized by means of a solution cast technique. The characterization techniques ... -
Synthesis of Silica-Based Nano Insulation Materials for Potential Application in Low-Energy or Zero Emission Buildings
(Journal article; Peer reviewed, 2017)Sacrificial polystyrene (PS) templates have been used for synthesis of silica-based nano insulation materials (NIM). The PS was synthesized by a simple procedure where parameters as polyvinylpyrrolidone/styrene ratio and ...