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VLE measurement and modelling of absorbents for absorption of CO2

Zahraee, Znar
Master thesis
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URI
http://hdl.handle.net/11250/2615714
Date
2017
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  • Institutt for kjemisk prosessteknologi [1240]
Abstract
Two promising solvents were studied for possible use as absorbents in CO2 post

combustion capture. The two solvents tested were 3-(Diethylamino)-1,2-propanediol

(DEA-12-PD) and 1-(2-Hydroxyethyl)piperidine (12-HEPP). A third amine N-tert-

Butyldiethanolamine (N-tBDEA) was also tested for another project and compared

with the two main amines.

Ebulliometer was used for measurements of pure DEA-12-PD and 12-HEPP,

and then used in regression of the Antoine equations. The plot of the Antoine

equations showed that 12-HEPP is the most volatile, while N-tBDEA is the least

volatile compound, but all the amines tested were less volatile than MEA. VLE

measurements of binary amine and water systems were also performed, and samples

were taken. The samples were analyzed and quantified by amine titration.

The Antoine equations and NRTL model of the measured VLE data were carried

out by the in-house program, Parafinder. The model required critical properties,

which were estimated from the Joback method, since those properties were

not available experimentally. The result of the NRTL model were evaluated by

the AARD of the total pressure. The AARD provided the fitness of the model to

the experimental data. The AARD of the total pressure for DEA-12-PD, 12-HEPP

and N-tBDEA are respectively 1.82 %, 2.46 % and 1.73 %.
Publisher
NTNU

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